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生态学杂志 ›› 1996, Vol. ›› Issue (4): 70-73.

• 研究报告 • 上一篇    下一篇

水、土壤及植物样品中1,2,4-三氯苯的提取和GC测定

张海荣, 区自清, 任丽萍, 张颜, 何耀武   

  1. 中国科学院沈阳应用生态研究所, 110015
  • 收稿日期:1996-04-17 出版日期:1996-08-10
  • 基金资助:
    国家自然科学基金;中国科学院“八五”重点科研项目;UNESCO中德国际合作CERP计划资助项目

Extraction of 1,2,4-trichlorobenzene from Water, Soil and Plant Tissue and Its Analysis on Gas Chromatography

Zhang Hairong, Ou Ziqing, Ren Liping, Zhang Yan, He Yaowu   

  1. Institute of Applied Ecology, Chinese Academy of Sciences, Shenyang 110015
  • Received:1996-04-17 Online:1996-08-10

关键词: 铜陵, 浮游植物, 群落结构, 重金属

Abstract: Ultrasonic extraction was used in the study on the analysis of 1,2,4-trichlorobenzene. In the study, 1,2,4-TCB in water samples was extracted with n-hexane whereas that in soil and plant, with mixture of n-hexanc and acetone at 9: 1. In all experiment, extractant of 15-25ml and an extraction time of 2h were performed. The recoveries of 1,2,4-trichlorobenzene from water, soil and plant (tissue stem and foliage of alfalfa and rice grain) were found to be more than 85%, 65% and 62%, respectively. The method was simple, sensitive and reliable for the analysis of 1,2,4-TCB, which is a volatile chemical, with low reagent demand, and applicable in the analysis of other chlorobenzenes in environment.

Key words: Tongling, phytoplankton, community structure, heavy metal.